3-Pyridin-3-ylpropanoyl chloride → 5-formyl-6-methoxy-3'-nitro-N-(3-pyridin-3-ylpropanoyl)-biphenyl-3-sulfonamide

HRID 1752921Notes

Reaction equation

HRID 1752921 reaction equation
[CH:1]([C:3]1[CH:4]=[C:5]([S:20]([NH2:23])(=[O:22])=[O:21])[CH:6]=[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([N+:17]([O-:19])=[O:18])[CH:12]=2)[C:8]=1[O:9][CH3:10])=[O:2].[N:24]1[CH:29]=[CH:28][CH:27]=[C:26]([CH2:30][CH2:31][C:32](Cl)=[O:33])[CH:25]=1>>[CH:1]([C:3]1[CH:4]=[C:5]([S:20]([NH:23][C:32](=[O:33])[CH2:31][CH2:30][C:26]2[CH:25]=[N:24][CH:29]=[CH:28][CH:27]=2)(=[O:22])=[O:21])[CH:6]=[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([N+:17]([O-:19])=[O:18])[CH:12]=2)[C:8]=1[O:9][CH3:10])=[O:2]

Participants

3

Reactant 2

HCID 149870663-Pyridin-3-ylpropanoyl chlorideHCID 866077105-Formyl-6-methoxy-3'-nitro-biphenyl-3-sulfonamide

Product 1

HCID 866077315-formyl-6-methoxy-3'-nitro-N-(3-pyridin-3-ylpropanoyl)-biphenyl-3-sulfonamide

Procedure

Proceeding as in Reference 21, but substituting 5-formyl-6-methoxy-3′-nitro-biphenyl-3-sulfonamide and 3-pyridin-3-ylpropanoyl chloride, gave 5-formyl-6-methoxy-3′-nitro-N-(3-pyridin-3-ylpropanoyl)-biphenyl-3-sulfonamide.

Sources & evidence

ORD record
ord-b4d769019e0d4a1a9cbca4a4d7c25d5d
Source dataset
uspto-grants-2015_10
Patent number
US09162986B2

Reaction notes

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