HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 11210968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | (Diethylamino)sulfur trifluoride | HCID 123472 | — |
| Reactant | Tedizolid | HCID 11234049 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11210968 | HCID 11210968 | 75.5% |
Reaction Steps
In 5 ml of methylenechloride was dissolved 100 mg of the compound 10. The solution was added with 43 mg of diethylaminosulfurtrifloride (DAST) and 0.078 ml of triethylamine and then stirred for 24 hours. After being concentrating, the reaction mixture was purified by column chromatography to obtain the title compound 75 mg. Yield 75%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163043B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-2e3951cdae9b4b9cbee273fd33355ceb |
| Source note | uspto-grants-2015_10 |