反应详情

温度

220 °C

A mixture of 9.8 g (18 mmol) of 6,14-dimethoxyditriphenyleno[2,3-b:2′,3′-d]thiophene, 31.2 g (270 mmol) of pyridine hydrochloride, was degassed and placed under nitrogen, and then heated at 220° C. for 6 h, the mixture was allowed to cool to room temperature and water was added. The resulting solid was filtered off, washed with water, and dried under high vacuum to give the product (8.2 g, 15.8 mmol, 88%).

1. customwas degassed
2. temperatureto cool to room temperature
3. additionwater was added
4. filtrationThe resulting solid was filtered off
5. washwashed with water
6. customdried under high vacuum