Potassium Carbonate → HCID 71682836, compound

Participants

Reaction Steps

31.5 mg (0.228 mmol) of potassium carbonate were added to 36.0 mg (0.076 mmol) of 2-methoxy-N-(1-methyl-1H-tetrazol-5-yl)-3-[S-methyl-N-(trifluoroacetyl)sulfonimidoyl]-4-(trifluoromethyl)benzamide in 5 ml of methanol. The mixture was stirred at RT for 30 minutes. For work-up, the solvent was removed at a temperature of at most 30° C. on a rotary evaporator. The residue was taken up in water and the mixture was extracted with dichloromethane. A drop of glacial acetic acid was then added to the aqueous phase, and the mixture was extracted twice with dichloromethane. On a rotary evaporator, the aqueous phase was then freed from the solvent at a temperature of at most 30° C. The residue was stirred with dichloromethane and then combined with the organic phases isolated above. The solvent was removed on a rotary evaporator, and 20 mg of product were isolated as residue.

Provenance & Evidence