1-Bromo-3-methylbutane → HCID 60195194, compound

HRID 1753755Notes

Reaction equation

HRID 1753755 reaction equation
[CH3:1][C:2]1[C:14]2[NH:13][C:12]3[C:7](=[CH:8][CH:9]=[C:10]([OH:15])[CH:11]=3)[C:6]=2[CH:5]=[CH:4][N:3]=1.Br[CH2:17][CH2:18][CH:19]([CH3:21])[CH3:20]>>[CH3:1][C:2]1[C:14]2[N:13]([CH2:17][CH2:18][CH:19]([CH3:21])[CH3:20])[C:12]3[C:7](=[CH:8][CH:9]=[C:10]([O:15][CH2:4][CH2:5][CH:6]([CH3:7])[CH3:14])[CH:11]=3)[C:6]=2[CH:5]=[CH:4][N:3]=1

Participants

3

Reactant 2

HCID 78911-Bromo-3-methylbutaneHCID 178432657HCID 178432657, compound

Product 1

HCID 60195194HCID 60195194, compoundYield 69%

Procedure

The title compound was synthesized from 1-methyl-7-hydroxy-β-carboline (1.504 g, 4.770 mmol) in presence of 1-bromo-3-methylbutane (1.440 g, 9.520 mmol) as described here above.

Sources & evidence

ORD record
ord-507eaf522eb3486e9ae662dac39dec27
Source dataset
uspto-grants-2015_10
Patent number
US09168247B2

Reaction notes

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