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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1753845Generated: October 28, 2026

Hydrochloric Acid → HCID 136330930, compound

https://huagongshe.com/reaction/1753845

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 136399885HCID 136399885—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 136330930HCID 136330930—

Reaction Steps

10 mg (0.02 mmol) of the compound from Example 177 are stirred with a 4 N solution of hydrogen chloride in dioxane at RT for 2 h. Thereafter, the solvent is decanted off and the solid is stirred in tert-butyl methyl ether three times in succession and the solvent is decanted off each time. The solid which remains is dried under a high vacuum.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09168249B2
Source datasetuspto-grants-2015_10
ORD IDord-695c5da9fa00480591ba89b2a9ee23e2
Source noteuspto-grants-2015_10