HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 136330930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 136399885 | HCID 136399885 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 136330930 | HCID 136330930 | — |
Reaction Steps
10 mg (0.02 mmol) of the compound from Example 177 are stirred with a 4 N solution of hydrogen chloride in dioxane at RT for 2 h. Thereafter, the solvent is decanted off and the solid is stirred in tert-butyl methyl ether three times in succession and the solvent is decanted off each time. The solid which remains is dried under a high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09168249B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-695c5da9fa00480591ba89b2a9ee23e2 |
| Source note | uspto-grants-2015_10 |