HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodobenzaldehyde → 4-(3-Iodo-benzyl)-piperazine-1-carboxylic acid phenylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodobenzaldehyde | HCID 252610 | — |
| Reactant | N-phenylpiperazine-1-carboxamide | HCID 7015289 | — |
| Product | 4-(3-Iodo-benzyl)-piperazine-1-carboxylic acid phenylamide | HCID 24020419 | — |
Reaction Steps
The title compound was prepared from piperazine-1-carboxylic acid phenylamide and 3-iodobenzaldehyde. 1H NMR (400 MHz, CDCl3): 7.71 (s, 1H), 7.62-7.60 (m, 1H), 7.36-7.26 (m, 5H), 7.09-7.01 (m, 2H), 6.33 (s, 1H), 3.52-3.48 (m, 6H), 2.49-2.46 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09169224B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-b7c2cd5c512e44008681a3d85f2fab28 |
| Source note | uspto-grants-2015_10 |