Ammonium dithiocarbamate → HCID 178480225, compound

HRID 1754239Notes

Reaction equation

HRID 1754239 reaction equation
[C:1](=[S:4])([S-:3])[NH2:2].[NH4+].[Br-].[Br:7][CH2:8][C:9]([C:11]1[CH:16]=[CH:15][N+:14]([CH3:17])=[CH:13][CH:12]=1)=O>CO>[Br-:7].[CH3:17][N+:14]1[CH:15]=[CH:16][C:11]([C:9]2[N:2]=[C:1]([SH:3])[S:4][CH:8]=2)=[CH:12][CH:13]=1

Participants

4

Reactant 2

HCID 11083854Ammonium dithiocarbamateHCID 89428956HCID 89428956, compound

Product 1

HCID 178480225HCID 178480225, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

0.69 g Ammonium dithiocarbamate were dissolved in 10 ml MeOH and 1.47 g 4-(2-bromoacetyl)-1-methylpyridinium bromide were added. After 2 h at ambient temperature the mixture was refluxed. After cooling the precipitate was filtered, washed with MeOH and dried.

Workup

  1. temperatureAfter cooling the precipitate
  2. filtrationwas filtered
  3. washwashed with MeOH
  4. customdried

Sources & evidence

ORD record
ord-a8470407e0a849e28e359849b1a8c0d7
Source dataset
uspto-grants-2015_10
Patent number
US09169239B2

Reaction notes

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