Trifluoroacetic acid → HCID 86700096, compound

Participants

Reaction Steps

Following the procedure as described in Example 11, except using the material from Example 24 (1.15 g, 2.66 mmol), CH2Cl2 (50 mL), TFA (5 mL, 64.9 mmol) and stirring at room temp for 18 h, 1.38 g of the title compound (quantitative yield) is obtained as a white solid as a mono TFA salt. LC/MS (Condition A): ret. T=2.86 min, (M+H)+ 376.13, and ret. T=3.03 min, (M+H)+ 376.13.

Provenance & Evidence