Sodium borohydride → HCID 86700115, compound

Participants

Reaction Steps

Following the procedure as described in Example 32, except using the material from Example 75 (106 mg, 0.119 mmol), EtOH/H2O (4:1) (4 mL), sodium borohydride (32.7 mg, 0.864 mmol) and stirring at room temp for 1 h, the title compound is isolated (quantitative yield) that is used crude in the next step. LC/MS (Condition A): ret. T=2.51 min, (M+H)+ 664.46.

Provenance & Evidence