Sodium borohydride → HCID 86700120, compound

Participants

Reaction Steps

Following the procedure as described in Example 32, except using material from Example 87 (16 mg, 0.014 mmol), EtOH/H2O (4:1) (5 mL), sodium borohydride (6.3 mg, 0.167 mmol) and stirring at room temp for 2.5 h, the title compound is isolated (quantitative yield) that is used crude in the next step. LC/MS (Condition A): ret. T=3.37 min, (2M+Na) 1005.75.

Provenance & Evidence