Sodium borohydride → HCID 86700123, compound

Participants

Reaction Steps

Following the procedure as described in Example 32, except using material from Example 73 (2.5 mg, 5.01 μmol), EtOH/H2O (4:1) (500 μlit), sodium borohydride (1.1 mg, 29.0 μmol) and stirring at room temp for 40 min, the title compound is isolated (quantitative yield) and is used crude in the next step. LC/MS (Condition A): ret. T=2.22 min, (M+H)+ 501.29.

Provenance & Evidence