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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1755507Generated: November 4, 2026

HCID 10904453, compound → HCID 117601866, compound

https://huagongshe.com/reaction/1755507

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10904453HCID 10904453—
ReactantHCID 89561323HCID 89561323—
CatalystPalladiumHCID 23938—
ProductHCID 117601866HCID 11760186672%

Reaction Steps

This product is synthesised from 2,7-dibromo-3.8-dioctyl-4,9-dihydro-s-indaceno[1,2-b:5,6-b′]dithiophene-4,9-dione (FL128, 0.65 g, 0.96 mmol) and 3-octyl-5-trimethylstannylthiophene (2.5 eq.) according to the Stille palladium catalysed coupling method as described previously. After which, the product is purified on chromatography column (silica gel, hexane/CHCl3, 7:3) to give 0.62 g (72%) of a green-blue solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09171676B2
Source datasetuspto-grants-2015_10
ORD IDord-db5cde928af2486fa4520cf62fc0c07e
Source noteuspto-grants-2015_10