HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10904453, compound → HCID 117601866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10904453 | HCID 10904453 | — |
| Reactant | HCID 89561323 | HCID 89561323 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 117601866 | HCID 117601866 | 72% |
Reaction Steps
This product is synthesised from 2,7-dibromo-3.8-dioctyl-4,9-dihydro-s-indaceno[1,2-b:5,6-b′]dithiophene-4,9-dione (FL128, 0.65 g, 0.96 mmol) and 3-octyl-5-trimethylstannylthiophene (2.5 eq.) according to the Stille palladium catalysed coupling method as described previously. After which, the product is purified on chromatography column (silica gel, hexane/CHCl3, 7:3) to give 0.62 g (72%) of a green-blue solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09171676B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-db5cde928af2486fa4520cf62fc0c07e |
| Source note | uspto-grants-2015_10 |