HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ceric ammonium nitrate → 2-Hydroxy-2-methyl-n-propyl-4-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dienyl)butanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ceric ammonium nitrate | HCID 180504 | — |
| Reactant | 6-hydroxy-2,5,7,8-tetramethyl-N-propylchroman-2-carboxamide | HCID 67262969 | — |
| Product | 2-Hydroxy-2-methyl-n-propyl-4-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dienyl)butanamide | HCID 42598874 | — |
Reaction Steps
Oxidation as described in protocol B, using 90.6 mg (0.311 mmol) of 6-hydroxy-2,5,7,8-tetramethyl-N-propylchroman-2-carboxamide and 374.9 mg CAN (0.684 mmol) yielded 2-hydroxy-2-methyl-N-propyl-4-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dienyl)butanamide as a yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09169196B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-5e7d1291d29c47b1aaf809a44800f9c3 |
| Source note | uspto-grants-2015_10 |