HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ceric ammonium nitrate → HCID 42599130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ceric ammonium nitrate | HCID 180504 | — |
| Reactant | 6-hydroxy-N-(5-hydroxypentyl)-2,5,7,8-tetramethylchroman-2-carboxamide | HCID 67262996 | — |
| Product | HCID 42599130 | HCID 42599130 | 92.3% |
Reaction Steps
Oxidation as described in protocol B, using 96 mg (0.286 mmol) of 6-hydroxy-N-(5-hydroxypentyl)-2,5,7,8-tetramethylchroman-2-carboxamide and 345 mg CAN (0.629 mmol) yielded 92.8 mg of 2-hydroxy-N-(5-hydroxypentyl)-2-methyl-4-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dienyl)butanamide as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09169196B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-86893dc11d2748e58fd10c51fcc82e53 |
| Source note | uspto-grants-2015_10 |