HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ceric ammonium nitrate → HCID 42599385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ceric ammonium nitrate | HCID 180504 | — |
| Reactant | HCID 67262914 | HCID 67262914 | — |
| Product | HCID 42599385 | HCID 42599385 | 90.5% |
Reaction Steps
Oxidation as described in protocol B, using 3.50 g (11.93 mmol) of (S)-6-hydroxy-N-(2-hydroxyethyl)-2,5,7,8-tetramethylchroman-2-carboxamide and 13.73 g CAN (25.06 mmol) yielded 3.341 g of (S)-2-hydroxy-N-(2-hydroxyethyl)-2-methyl-4-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dienyl)butanamide as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09169196B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-4592fda7ecbb4e05979881f5c2913c6d |
| Source note | uspto-grants-2015_10 |