HCID 54437313, compound → HCID 54058363, compound

Participants

Reaction Steps

A mixture of the benzylic alcohol of Step 7 (1.176 g, 2.54 mmol) and activated MnO2 (4.6 g, 20 equiv.) in 25 mL of EtOAc was stirred at room temperature for 4 hr. Another batch of MnO2 (1.1 g) was added and the mixture was stirred 20 min. It was filtered through celite to afford 1.014 g (87%) of the title aldehyde.

Provenance & Evidence