HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroacetophenone → 2-Methoxymethyl-3-methyl-7-phenacyl pyrrolo[2,3-b]pyridine. Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroacetophenone | HCID 10757 | — |
| Reactant | 2-Methoxymethyl-3-methylpyrrolo[2,3-b]pyridine | HCID 19916813 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 2-Methoxymethyl-3-methyl-7-phenacyl pyrrolo[2,3-b]pyridine. Hydrochloride | HCID 131719076 | 20.4% |
Reaction Steps
A solution of 0,13 g (0,74 mmol) 2-methoxymethyl-3-methylpyrrolo[2,3 -b]pyridine and 0,16 g (1,1 mmol) phenacyl chloride in 20 ml acetonitrile was refluxed for 15 h. Working up in the same manner as ex. 17 gave 0,05 g (20%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-38cda9a4975e4f91a3cf99d084057564 |
| Source note | uspto-grants-1995_08 |