Acetonitrile → HCID 70347101, compound

Participants

Reaction Steps

A solution of 73 mg (0,5 mmol) 2,3 dimethylpyrrolo[2,3-b]pyridine and 122 mg (0,5 mmol) of (2-bromoethyl)acetanilide in 2 ml acetonitrile was refluxed for 10 h. The solvent was evaporated and the crude product was treated with 5 ml petroleum ether:ether 1:1 and the insoluble fraction was treated with ether. The etheral layer was separated from the oily residue, which crystallized from acetronitrile and gave 15 mg (7,7%) of the title compound.

Provenance & Evidence