HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 23207147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 19916777 | HCID 19916777 | — |
| Product | HCID 23207147 | HCID 23207147 | — |
Reaction Steps
The title compound was prepared from 5-chloro-3-cyanomethyl-2-methyl-7-phenacylpyrrolo[2,3-b]pyridine (example 33) and NaBH4 on a 0.33 mmol scale according to the procedure described in example 11. Chromatography of the crude material (silica, CH2Cl2 /MeOH; 96/4) afforded 45 mg (42%) pure product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-3e24cd12498b43c09ac4cd001a1a3717 |
| Source note | uspto-grants-1995_08 |