HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178520568, compound → HCID 178520567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178520568 | HCID 178520568 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Tetrachloroethylene | HCID 31373 | — |
| Product | HCID 178520567 | HCID 178520567 | — |
Reaction Steps
5,5 g of 4-(1-hydroxy-5-phenylpentyl)-1H-imidazole and 7,0 g of manganese dioxide are refluxed stirring in tetrachloroethylene for four hours. The reaction mixture is filtered and the filtrate is evaporated to dryness. Water is added and the product is extracted into methylene chloride. The combined extracts are washed with water and evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439928 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-3927a211e2ce4a5db43b17ed50c0c468 |
| Source note | uspto-grants-1995_08 |