HCID 15341803, compound → HCID 15341818, compound

HRID 1756207Notes

Reaction equation

HRID 1756207 reaction equation
[OH:1][C:2]1[C:10]([CH2:11][CH:12]=[CH2:13])=[C:9]([OH:14])[CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5]>[Pd].C(O)C>[OH:1][C:2]1[C:10]([CH2:11][CH2:12][CH3:13])=[C:9]([OH:14])[CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5]

Participants

4

Reactant 1

HCID 15341803HCID 15341803, compound

Product 1

HCID 15341818HCID 15341818, compoundYield 74%

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

2,4-Dihydroxy-3-(2-propenyl)benzamide (575 mg) and 125 ml of ethanol was hydrogenated at 5 psi, room temperature, using 4% Pd/C catalyst for 3 hours. The solvent was removed under vacuum to give the product as an oil (4.25 mg, 74%).

Workup

  1. customwas hydrogenated at 5 psi, room temperature
  2. customfor 3 hours
  3. customThe solvent was removed under vacuum

Sources & evidence

ORD record
ord-813866da66e14739b829e39805f2dc8e
Source dataset
uspto-grants-1995_08
Patent number
US05439937

Reaction notes

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