HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 2-(3-Carboxybenzoyl)-6-[(1E)-(3RS)-3-hydroxy-1-undecenyl]-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-(3-Methoxycarbonylbenzoyl)-6-[(1E)-(3RS)-3-hydroxy-1-undecenyl]-pyridine | HCID 15661741 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(3-Carboxybenzoyl)-6-[(1E)-(3RS)-3-hydroxy-1-undecenyl]-pyridine | HCID 15661743 | 77.7% |
Reaction Steps
Under the conditions of example 2, 20 mg of 2-(3-methoxycarbonylbezoyl)-6-[(1E)-(3RS)-3-hydroxy-1-undecenyl]-pyridine in 1 ml of methanol is saponified with 2 ml of 1 n sodium hydroxide solution and worked up. 15 mg of the title compound is obtained as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05440044 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-95d104c54b43436f837b5e958baba325 |
| Source note | uspto-grants-1995_08 |