HCID 19068273, compound → HCID 21474579, compound

HRID 1756434Notes

Reaction equation

HRID 1756434 reaction equation
[C:1]12([C:11]3[CH:12]=[C:13]([OH:19])[CH:14]=[CH:15][C:16]=3[O:17][CH3:18])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[Cl:20][C:21]([O-])=[O:22]>>[Cl:20][C:21]([O:19][C:13]1[CH:14]=[CH:15][C:16]([O:17][CH3:18])=[C:11]([C:1]23[CH2:2][CH:3]4[CH2:9][CH:7]([CH2:6][CH:5]([CH2:4]4)[CH2:10]2)[CH2:8]3)[CH:12]=1)=[O:22]

Participants

3

Reactant 2

HCID 19068273HCID 19068273, compoundHCID 21226386Carbonochloridate

Product 1

HCID 21474579HCID 21474579, compound

Procedure

In a manner similar to Example 17(a), starting with 6.45 g (25 mmol) of 3-(1-adamantyl)-4-methoxyphenol, 5 g (62%) of the expected chloroformate, melting point 87°-89° C., are obtained.

Workup

  1. customare obtained

Sources & evidence

ORD record
ord-2d7ea5952ab3442580af3ffab53d60e0
Source dataset
uspto-grants-1995_08
Patent number
US05439925

Reaction notes

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