HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Allyloxycarbonyl)benzoic acid → Allyl 4-{[1-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)ethyloxy]carbonyl}benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Allyloxycarbonyl)benzoic acid | HCID 18349855 | — |
| Reactant | 1-(5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethanol | HCID 21474499 | — |
| Product | Allyl 4-{[1-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)ethyloxy]carbonyl}benzoate | HCID 21474484 | — |
Reaction Steps
In a manner similar to Example 4(c), by reaction of 2.1 g (10 mmol) of 4-(allyloxycarbonyl)benzoic acid with 2.3 g (10 mmol) of 1-(5,6,7,8-tetrahydro -5,5,8,8-tetramethyl-2-naphthyl)ethanol, 3.2 g (76%) of the expected allyl ester are obtained in the form of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439925 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-890ca3f21e244234907408ba29f95bd4 |
| Source note | uspto-grants-1995_08 |