3-Tert-butyl-4-methoxybenzoyl chloride → HCID 21474569, compound

HRID 1756459Notes

Reaction equation

HRID 1756459 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8](Cl)=[O:9])([CH3:4])([CH3:3])[CH3:2].[OH:16][CH2:17][C:18]1[S:22][C:21]([C:23]([O:25][CH2:26][CH:27]=[CH2:28])=[O:24])=[CH:20][CH:19]=1>>[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8]([O:16][CH2:17][C:18]1[S:22][C:21]([C:23]([O:25][CH2:26][CH:27]=[CH2:28])=[O:24])=[CH:20][CH:19]=1)=[O:9])([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 136335553-Tert-butyl-4-methoxybenzoyl chlorideHCID 21474497HCID 21474497, compound

Product 1

HCID 21474569HCID 21474569, compound

Procedure

In a manner similar to Example 1(d), by reaction of 1.6 g (7 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 1.4 g (7 mmol) of allyl 5-hydroxymethyl -2-thiophenecarboxylate, 1.5 g (55%) of allyl ester are obtained in the form of a slightly yellow oil.

Workup

  1. customare obtained in the form of a slightly yellow oil

Sources & evidence

ORD record
ord-941b4cf25a414e438474ad3dcbd9be22
Source dataset
uspto-grants-1995_08
Patent number
US05439925

Reaction notes

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