HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloroisatoic anhydride → HCID 478575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloroisatoic anhydride | HCID 78480 | — |
| Reactant | 5-chloro-1H-indole-2,3-dione | HCID 87203 | — |
| Reactant | 5-Fluoroisatin | HCID 236566 | — |
| Product | HCID 478575 | HCID 478575 | — |
Reaction Steps
Using the procedure in Example 12 and substituting isatoic anhydride for 5-chloroisatoic anhydride and 5-chloroisatin for 5-fluoroisatin gave the title compound in 39% crude yield: mp 295°-296° C.; 1H NMR (300 MHz, DMSO-d6) δ 8.46-8.53 (m, 1H), 8.33 (d, 1H), 7.96 (d, 2H), 7.69-7.84 (m, 3H); MS (M+H)+ 283.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05441955 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-847f56460de84e28867a6e107e7ba994 |
| Source note | uspto-grants-1995_08 |