HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatin → HCID 478672, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatin | HCID 7054 | — |
| Reactant | 2-Aminonicotinic acid | HCID 72930 | — |
| Reactant | 5-Fluoroisatin | HCID 236566 | — |
| Product | HCID 478672 | HCID 478672 | 6% |
Reaction Steps
Using the procedure in Example 56, and substituting 3-aminopyrazine-2-carboxylic acid for 2-aminonicotinic acid and 5-fluoroisatin for isatin gave 79 mg (6%) of the title compound: mp 336° C. (dec); 1H NMR(DMSO-d6) δ 7.65-8.00 (m, 2H), 8.50 (s, 1H), 9.05-9.20 (m, 2H); MS (M+H)+ 269.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05441955 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-90242ca1d8024b3690d618536fe63623 |
| Source note | uspto-grants-1995_08 |