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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1756906Generated: October 28, 2026

Triethylamine → HCID 21469488, compound

https://huagongshe.com/reaction/1756906

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant1-BromododecaneHCID 8919—
ReactantHCID 178509541HCID 178509541—
SolventAcetonitrileHCID 6342—
ProductHCID 21469488HCID 21469488—

Reaction Steps

The tetrazole (b) obtained above (11.0 g; 0.067 moles) was dissolved in acetonitrile (150 mL) containing one equivalent of triethylamine (6.8 g; 0.067 moles). The solution was heated to reflux followed by the addition of 1-bromo dodecane (16.8 g; 0.067 moles). Isolation of the 2-isomer was achieved employing the same conditions described for Example 11.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05441975
Source datasetuspto-grants-1995_08
ORD IDord-83f5b5ae479044a0b12bf7765da7f688
Source noteuspto-grants-1995_08