Ethyl 2-bromoheptanoate → ethyl(+/-)-5-dodecyl-alpha-pentyl-2H-tetrazole-2-acetate
Reaction equation
[CH2:1]([C:13]1[NH:17][N:16]=[N:15][N:14]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].C(C1NN=NN=1)CCCCCCCCC.[CH2:33]([O:35][C:36](=[O:44])[CH:37](Br)[CH2:38][CH2:39][CH2:40][CH2:41][CH3:42])[CH3:34].BrC1C=CC=CC=1CC(OCC)=O>>[CH2:1]([C:13]1[N:14]=[N:15][N:16]([CH:37]([CH2:38][CH2:39][CH2:40][CH2:41][CH3:42])[C:36]([O:35][CH2:33][CH3:34])=[O:44])[N:17]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]Participants
5
Procedure
When in the general procedure of Example 71 an appropriate amount of 5-dodecyl-1H-tetrazole was substituted for 5-decyl-1H-tetrazole and an appropriate amount of ethyl-2-bromoheptanoate was substituted for ethyl 2-bromophenylacetate, the title compound was obtained.
Sources & evidence
- ORD record
- ord-f89d62d5cff54b389e5793a7e4cf7c06
- Source dataset
- uspto-grants-1995_08
- Patent number
- US05441975
Reaction notes
Loading…