1-Octanol → HCID 53737560, compound

HRID 1757028Notes

Reaction equation

HRID 1757028 reaction equation
Br[C:2]1[N:7]=[CH:6][C:5]([Br:8])=[CH:4][N:3]=1.[CH2:9]([OH:17])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>>[CH2:9]([O:17][C:2]1[N:7]=[CH:6][C:5]([Br:8])=[CH:4][N:3]=1)[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 9571-OctanolHCID 109555882,5-Dibromopyrimidine

Product 1

HCID 53737560HCID 53737560, compound

Procedure

Analogously to the above procedure, 5.95 g of 2,5-dibromopyrimidine are reacted with 7.9 g of 1-octanol to give 2-octyloxy-5-bromopyrimidine. The product is purified by chromatography on silica gel.

Sources & evidence

ORD record
ord-63f07d2edff047968181926d994b00b3
Source dataset
uspto-grants-1995_08
Patent number
US05443754

Reaction notes

Loading…