Imidazole → HCID 86748902, compound

HRID 1757054Notes

Reaction equation

[C:1]([O-:4])(=[O:3])[CH3:2].[Ni+2:5].[C:6]([O-:9])(=[O:8])[CH3:7].[NH:10]1[CH:14]=[CH:13][N:12]=[CH:11]1>>[C:1]([O-:4])(=[O:3])[CH3:2].[Ni+2:5].[NH:10]1[CH:14]=[CH:13][N:12]=[CH:11]1.[NH:10]1[CH:14]=[CH:13][N:12]=[CH:11]1.[NH:10]1[CH:14]=[CH:13][N:12]=[CH:11]1.[NH:10]1[CH:14]=[CH:13][N:12]=[CH:11]1.[NH:10]1[CH:14]=[CH:13][N:12]=[CH:11]1.[NH:10]1[CH:14]=[CH:13][N:12]=[CH:11]1.[C:6]([O-:9])(=[O:8])[CH3:7]

Participants

Reactant 2

HCID 795Imidazole

HCID 9756Nickel Acetate

Product 1

HCID 86748902HCID 86748902, compoundYield 97.5%

Procedure

1 mole of nickel (II) acetate and 6 moles of imidazole were heated to 100° C. in a stirred reactor with thorough mixing at 200 to 400 rpm for 5 to 10 minutes to obtain a complex of hexa (imidazole) nickel (II) acetate with a 97.5% yield, based on the metal salt.

Workup

additionwith thorough mixing at 200 to 400 rpm for 5 to 10 minutes

Sources & evidence

ORD record: ord-9a21a13b20bc4ce28206a7277b4f514b
Source dataset: uspto-grants-1995_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05444030

Reaction notes

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