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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1757076Generated: October 28, 2026

HCID 53871764, compound → HCID 10649365, compound

https://huagongshe.com/reaction/1757076

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53871764HCID 53871764—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 10649365HCID 10649365112.6%

Reaction Steps

Diethyl 3-(3-(2-α-D-mannopyranosyloxyphenyl)phenyl)prop-1-enylphosphonate (0.46 g, 0.80 mmol) was dissolved in ethanol (25 ml) and hydrogenated (40 psi H2, 10% Pd/C) for 3 hours. The suspension was filtered through celite and the filtrate concentrated under reduced pressure to afford diethyl 3-(3-(2-α-D-mannopyranosyloxyphenyl)phenyl)propylphosphonate (0.46 g, quantitative).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05444050
Source datasetuspto-grants-1995_08
ORD IDord-14e4a4a21b9c41a5822c4c0441416ed8
Source noteuspto-grants-1995_08