HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53871764, compound → HCID 10649365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53871764 | HCID 53871764 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10649365 | HCID 10649365 | 112.6% |
Reaction Steps
Diethyl 3-(3-(2-α-D-mannopyranosyloxyphenyl)phenyl)prop-1-enylphosphonate (0.46 g, 0.80 mmol) was dissolved in ethanol (25 ml) and hydrogenated (40 psi H2, 10% Pd/C) for 3 hours. The suspension was filtered through celite and the filtrate concentrated under reduced pressure to afford diethyl 3-(3-(2-α-D-mannopyranosyloxyphenyl)phenyl)propylphosphonate (0.46 g, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05444050 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-14e4a4a21b9c41a5822c4c0441416ed8 |
| Source note | uspto-grants-1995_08 |