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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1757193Generated: October 31, 2026

Ethyl Acetate → HCID 22400396, compound

https://huagongshe.com/reaction/1757193

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl AcetateHCID 8857—
ReactantHCID 22400428HCID 22400428—
SolventDichloromethaneHCID 6344—
ProductHCID 22400396HCID 2240039671%

Reaction Steps

The procedure of Example 3(iv) was followed using 5-(2-chloro)ethyl-1-[(2-chlorophenyl)methyl]-2-propylthio-1H-imidazole hydrochloride in place of 5-chloromethyl-1-[(2chlorophenyl)methyl]2-propylthio-1H-imidazole hydrochloride. The title compound was obtained in 71% yield after chromatography over silica gel with a gradient of ethyl acetate in methylene chloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05444080
Source datasetuspto-grants-1995_08
ORD IDord-579b9e1c78fe4eb1a4605d5683f59c8b
Source noteuspto-grants-1995_08