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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1757299Generated: November 1, 2026

Z-DTrp-betaAla-OEt → DTrp-betaAla-OEt

https://huagongshe.com/reaction/1757299

Reaction equation

Participants

RoleNameHCIDCharge
ReactantZ-DTrp-betaAla-OEtHCID 131719105—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductDTrp-betaAla-OEtHCID 13171910699.8%

Reaction Steps

The compound obtained in (1) (650 mg) was dissolved in methanol (10 ml) and 10% Pd-C (118 mg) was added. The resulting mixture was vigorously stirred at room temperature under atmospheric pressure of hydrogen overnight. The catalyst was filtered off through Celite and the filtrate was concentrated under reduced pressure to give the product (450 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05444152
Source datasetuspto-grants-1995_08
ORD IDord-964d0991f98448b1b837a6dfb5f4b22f
Source noteuspto-grants-1995_08