HuagongsheHuagongshe Chemistry Print Report · For research reference only
Z-DTrp-betaAla-OEt → DTrp-betaAla-OEt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Z-DTrp-betaAla-OEt | HCID 131719105 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | DTrp-betaAla-OEt | HCID 131719106 | 99.8% |
Reaction Steps
The compound obtained in (1) (650 mg) was dissolved in methanol (10 ml) and 10% Pd-C (118 mg) was added. The resulting mixture was vigorously stirred at room temperature under atmospheric pressure of hydrogen overnight. The catalyst was filtered off through Celite and the filtrate was concentrated under reduced pressure to give the product (450 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05444152 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-964d0991f98448b1b837a6dfb5f4b22f |
| Source note | uspto-grants-1995_08 |