Trichloroacetyl chloride → HCID 178447928, compound

HRID 1757343Notes

Reaction equation

HRID 1757343 reaction equation
[CH2:1]([C@H:4]1[CH2:9][CH2:8][C@H:7]([CH:10]=[CH2:11])[CH2:6][CH2:5]1)[CH2:2][CH3:3].[Cl:12][C:13]([Cl:18])(Cl)[C:14](Cl)=[O:15]>C(OCC)C>[CH2:1]([C@H:4]1[CH2:5][CH2:6][C@H:7]([CH:10]2[CH2:11][C:14](=[O:15])[C:13]2([Cl:18])[Cl:12])[CH2:8][CH2:9]1)[CH2:2][CH3:3]

Participants

4

Reactant 2

HCID 6420Trichloroacetyl chlorideHCID 178455742HCID 178455742, compound

Product 1

HCID 178447928HCID 178447928, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A mixture of 0.25 mol of trans-4-propyl-1-vinylcyclohexane (prepared according to WO 88/02357) and 800 ml of diethyl ether is reacted with trichloroacetyl chloride in accordance with Example 1B.

Sources & evidence

ORD record
ord-a88264b322f3465d846652b0a5ba5584
Source dataset
uspto-grants-1995_08
Patent number
US05445764

Reaction notes

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