HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethyl 4-methoxyphenyl ketone → HCID 23371593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethyl 4-methoxyphenyl ketone | HCID 4965 | — |
| Reactant | 5-(Pyridin-4-yl)-3,6-dihydro-2H-1,3,4-thiadiazin-2-one | HCID 23371628 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23371593 | HCID 23371593 | 96.4% |
Reaction Steps
5-(4-Pyridyl)-3H,6H-1,3,4-thiadiazin-2-one (386 mg, 2 mmol) and 4'-methoxyphenacyl bromide (550 mg, 2.4 mmol) were dissolved in absolute ethanol (6 ml), refluxed for three hours and then stirred at room temperature overnight. The resulting precipitate was collected by filtration and washed with absolute ethanol to obtain the titled compound (814 mg) as light brown powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446042 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-86cc371cb75248abad973ccf53d37837 |
| Source note | uspto-grants-1995_08 |