HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Butadiene → 1,3-Butadiene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Butadiene | HCID 7845 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | 1,3-Butadiene | HCID 7845 | — |
| Product | HCID 86748943 | HCID 86748943 | — |
Reaction Steps
Butadiene was polymerized in a cyclohexane solvent with a polymerization catalyst of lithium n-butyl. Then, tetrahydrofuran was added as a vinylization agent, to polymerize butadiene, to obtain a butadiene-vinyl butadiene copolymer. The copolymer had a degree of vinylization of vinyl butadiene part of 60%. The polymer was hydrogenated to give a hydrogenatedblock copolymer having a hydrogenation ratio of 98%. This polymer was namedR-5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446092 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-ce83e16a659043f993d256b71fe55911 |
| Source note | uspto-grants-1995_08 |