N,N-Diethyl-1,3-propanediamine → HCID 10540994, compound

HRID 1757566Notes

Reaction equation

HRID 1757566 reaction equation
[Cl:1][C:2]1[CH:13]=[C:6]2[C:7]([O:9]C(=O)[NH:11][C:5]2=[CH:4][CH:3]=1)=O.[CH2:14]([N:16]([CH2:21][CH3:22])[CH2:17][CH2:18][CH2:19][NH2:20])[CH3:15]>O1CCOCC1>[NH2:11][C:5]1[CH:4]=[CH:3][C:2]([Cl:1])=[CH:13][C:6]=1[C:7]([NH:20][CH2:19][CH2:18][CH2:17][N:16]([CH2:21][CH3:22])[CH2:14][CH3:15])=[O:9]

Participants

4

Reactant 2

HCID 61011N,N-Diethyl-1,3-propanediamineHCID 784805-Chloroisatoic anhydride

Product 1

HCID 10540994HCID 10540994, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

A solution containing 4.00 grammes (20.3 mmoles) of 5-chloroisatoic anhydride in 25 ml of dioxane at room temperature is joined by 4.80 ml (30.4 mmoles) of 3-diethylamino- 1-propylamine.

Sources & evidence

ORD record
ord-0c63884e9f3f4061a89935651a41ce18
Source dataset
uspto-grants-1995_08
Patent number
US05446152

Reaction notes

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