HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethoxyphenyl methyl ketone → HCID 53851383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethoxyphenyl methyl ketone | HCID 14328 | — |
| Reactant | 3,4-Dihydroxy-5-nitrobenzaldehyde | HCID 5748957 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53851383 | HCID 53851383 | — |
Reaction Steps
The procedure described in Example 8 was repeated using 1.8 g of 3,4-dihydroxy-5-nitrobenzaldehyde and 18 g of 3',4'-dimethoxyacetophenone in 20 ml of methanol. Yield 1.7 g (50%), m.p. 206°-208° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446194 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-f006576f99964ee8af509a605f4a5fc9 |
| Source note | uspto-grants-1995_08 |