8-Oxononanoic acid → HCID 54344342, compound

HRID 1757631Notes

Reaction equation

HRID 1757631 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[C:9]=1[OH:10])[CH:5]=O.[O:14]=[C:15]([CH3:25])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22]([OH:24])=[O:23]>>[OH:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[C:9]=1[OH:10])[CH:5]=[C:16]([C:15](=[O:14])[CH3:25])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22]([OH:24])=[O:23]

Participants

3

Reactant 2

HCID 53129418-Oxononanoic acidHCID 57489573,4-Dihydroxy-5-nitrobenzaldehyde

Product 1

HCID 54344342HCID 54344342, compound

Procedure

The procedure described in Example 9 was repeated using 1.83 g of 3,4-dihydroxy-5-nitrobenzaldehyde and 1.72 g of 8-ketononanoic acid. Yield1.85 g (55%), yellow viscous oil.

Sources & evidence

ORD record
ord-57c7a8ccca5c4a099391fa63c46035fb
Source dataset
uspto-grants-1995_08
Patent number
US05446194

Reaction notes

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