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HRID1757636

反应详情

EQUATION

反应方程式

HRID 1757636 的结构方程式

REACTANTS

反应物

1
结构：CCCCCCCCCCCCCCOC(=O)CCCCc1cc(O)c(O)c([N+](=O)[O-])c1
HCID19389193

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCOC(=O)CCCCc1cc(OC(C)=O)c(OC(C)=O)c([N+](=O)[O-])c1
HCID19389212

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)OC(C)=O
溶剂HCID7918

Acetic anhydride

C4H6O3

PROCEDURE

实验过程

A solution containing 0.1 g of the product obtained in Example 29 in 2 ml of acetic anhydride was refluxed for 20 min. The solvent was evaporated invacuo and the residue crystallized from petroleum ether (b.p. 40° C.), m.p. 52°-54° C.

WORKUP

后处理

  1. temperaturewas refluxed for 20 min
  2. customThe solvent was evaporated invacuo
  3. customthe residue crystallized from petroleum ether (b.p. 40° C.), m.p. 52°-54° C.