HCID 19389224, compound → HCID 53677781, compound

HRID 1757652Notes

Reaction equation

HRID 1757652 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[C:9]([S:13]([CH3:16])(=[O:15])=[O:14])[C:10]=1[O:11][CH3:12])[CH:6]=O>CC(=O)CC>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:6]=[C:10]([CH3:9])[C:3](=[O:2])[CH3:4])[CH:8]=[C:9]([S:13]([CH3:16])(=[O:15])=[O:14])[C:10]=1[O:11][CH3:12]

Participants

3

Reactant 1

HCID 19389224HCID 19389224, compound

Product 1

HCID 53677781HCID 53677781, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

The procedure described in Example 8 was repeated using 2.44 g of 3,4-dimethoxy-5-methylsulfonylbenzaldehyde and 1.0 g of 2-butanone. Yield 2.0 g (63%), viscous oil.

Sources & evidence

ORD record
ord-e2dd57d83af04969ad19ba78030e3b88
Source dataset
uspto-grants-1995_08
Patent number
US05446194

Reaction notes

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