HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 19389214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 3,5-Dinitrocatechol | HCID 3870203 | — |
| Product | HCID 19389214 | HCID 19389214 | — |
Reaction Steps
A mixture containing 2.0 g of 3,5-dinitrocatechol in 5 ml of benzoylchloride was cooked for 4 hours in 100° C. When cooled petroleum ether (b.p. 40° C.) was added and the product was filtered and washed with petroleum ether. The raw product was crystallizedfrom ethanol. Yield 2.5 g (82%), m.p. 150°-152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446194 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-3ec49391ca9a448ea0c27ee045876fe0 |
| Source note | uspto-grants-1995_08 |