HCID 19389044, compound → HCID 19389086, compound

Participants

Reaction Steps

A mixture of 1.65 g of N-(3,5-didecylphenyl)-N-[2-(phenylmethoxy)-2-oxoethyl]glycine phenylmethylester and 0.5 g of 10% palladium on carbon in 100 ml of THF was shaken under an initial hydrogen pressure of 53 psi for 5 hours. The catalyst wasremoved by filtration and the filtrate was concentrated at reduced pressureto a solid which was recrystallized from methanol-water to give 0.98 g (81%yield, mp 78°-81°) of N-(carboxymethyl)-N-(3,5-didecylphenyl)glycine.

Provenance & Evidence