HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → N-(2-methoxy-2-oxoethyl)-N-[3,5-bis(decyloxy)phenyl]glycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-[3,5-Bis(decyloxy)phenyl]2,6-morpholinedione | HCID 19389079 | — |
| Product | N-(2-methoxy-2-oxoethyl)-N-[3,5-bis(decyloxy)phenyl]glycine | HCID 19388975 | — |
Reaction Steps
A solution of 0.469 g of 4-[3,5-bis(decyloxy)phenyl]2,6-morpholinedione in 50 ml of methanol was warmed to 50° and then was left at room temperature for 17 hours. The solvent was removed at reduced pressure to give 0.44 g, mp 61°-62° of pure N-(2-methoxy-2-oxoethyl)-N-[3,5-bis(decyloxy )phenyl]glycine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05446189 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-3907d8f37ffb4631b77ba0b2af77e90c |
| Source note | uspto-grants-1995_08 |