HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dinitrophenol → 1,4-Bis-(2',4'-dinitrophenoxy)-butan-2,3-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dinitrophenol | HCID 1493 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,4-Dibromo-2,3-butanediol | HCID 98512 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1,4-Bis-(2',4'-dinitrophenoxy)-butan-2,3-diol | HCID 20510280 | — |
Reaction Steps
A mixture of 19.2 gm (0.1 mol) of 2,4-dinitrophenol (96%), 12.4 gm (0.05 mol) of 1,4-dibromo-butan-2,3-diol, and 6.9 gm (0.05 mol) of potassium carbonate was refluxed for six hours in 20 ml of diethyleneglycoldimethyl ether. After cooling, the product was removed by suction, washed with water, and dried. The intermediate obtained melted at 207°-210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04371370 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-9adbc0befa4941328337ad9678f1cea9 |
| Source note | uspto-grants-1983_02 |