HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12822120, compound → HCID 54253370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12822120 | HCID 12822120 | — |
| Reactant | HCID 12822121 | HCID 12822121 | — |
| Product | HCID 54253370 | HCID 54253370 | 57% |
Reaction Steps
Following a procedure analagous to that of Example 1(b) but using respectively 2,6-diethoxy-3-(α-ethoxy-2-chlorobenzyl)tetrahydropyran and 2,6-diethoxy-3-(α-ethoxy-4-methoxybenzyl)tetrahydropyran there was obtained respectively 2-(2-chlorobenzylidene)glutaraldehyde, b.p. 155° C. (0.8 mm), yield: 57%; and 2-(4-methoxybenzylidene)glutaraldehyde, b.p. 175° C. (1.0 mm), yield 61%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04371547 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-2610d7631c144372b68f10831a69e0aa |
| Source note | uspto-grants-1983_02 |