HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20510885, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,5-Dichloropyridine | HCID 27685 | — |
| Reactant | 1,2-Benzenedithiol | HCID 69370 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20510885 | HCID 20510885 | — |
Reaction Steps
In 50 ml of stirred dimethylformamide, a mixture of 3.0 grams (0.02 mole) dimercaptobenzene, 7.0 grams potassium carbonate, and 7.0 grams of 2,5-dichloropyridine is heated at 80° for 5 hours. Thereafter pouring into excess H2O, the mixture is extracted with ethyl ether (200 ml) and washed with H2O, saturated NaHCO3, and brine, dried (MgSO4), and evaporated to yield the crude product which can be recrystallized from 1-chlorobutane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04371736 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-561892268755477384fac0833d9329b9 |
| Source note | uspto-grants-1983_02 |