HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triglycidylglycerol → 1,2,3-Tris[3-(4-benzoyloxy-2,2,6,6-tetramethylpiperidino)-2-hydroxypropoxy]propane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triglycidylglycerol | HCID 25795 | — |
| Reactant | 2,2,6,6-Tetramethyl-4-piperidyl benzoate | HCID 579967 | — |
| Product | 1,2,3-Tris[3-(4-benzoyloxy-2,2,6,6-tetramethylpiperidino)-2-hydroxypropoxy]propane | HCID 20510591 | — |
Reaction Steps
A mixture of 10.1 g of 4-benzoyloxy-2,2,6,6-tetramethylpiperidine and 2.6 g of glycerol tris(2,3-epoxypropyl)ether was reacted following the procedure described in Example 5 to give the desired Compound No. 115 in the form of a white vitreous solid having an Rf value of 0.87 on thin-layer chromatography on silica gel developed with a 4:1 by volume mixture of ethyl acetate and triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04371644 |
| Source dataset | uspto-grants-1983_02 |
| ORD ID | ord-18a88326651540f8aad31d676b6135b5 |
| Source note | uspto-grants-1983_02 |